Factors Affecting the Forensic Examination of Automotive Lubricating Oils

• Autores: Ryan Hibbard, John V. Goodpaster, Michelle R. Evans
• Localización: Journal of forensic sciences, ISSN-e 1556-4029, ISSN 0022-1198, Vol. 56, Nº. 3, 2011, págs. 741-753
• Idioma: inglés
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• Resumen

  • Keywords:forensic science;chemometrics;high-temperature gas chromatography/mass spectrometry;lubricating oils;motor oils;power steering fluid Abstract: Lubricating oil comparisons impact a variety of forensic investigations, including cases where oil was transferred from a suspect vehicle to the crime scene or victim. In this study, high-temperature gas chromatography/mass spectrometry was used to examine the influence of oil mixtures and oil changes over time on the comparison of known and questioned lubricating oils. Varying concentrations of oil mixtures were prepared and showed the potential for identifying individual components. Motor oils from 18 automobiles monitored over a 2-month period did not demonstrate significant changes in the chromatographic data. Chemometric analysis of motor oil mass spectral data provided little information regarding differentiation of, or changes in, the samples. Power steering fluid (PSF) from a naturally occurring leak collected from several locations was consistent with the PSF in the automobile�s reservoir, and the PSF composition did not change over time.