Resumen de The Synthesis and Reactions of Nickel(III) Stabilized by a Nitrogen-Donor Macrocycle

David E. Berry, Suzanne Girard, Alexander McAuley

• This experiment describes the synthesis of 1,4,8,11-tetraazacyclotetradecane and its nickel(II and III) complexes avoiding the use of percholrate anion. The paramagnetic effects in solution and solid state are described for the nickel(III) dihalo derivatives along with a spectrophotometric study.