Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate

• Autores: Jason A. Halfen, Victor G. Young
• Localización: Chemical communications, ISSN 1359-7345, Nº. 23, 2003, págs. 2894-2895
• Idioma: inglés
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• Resumen

  • facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(II) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle