A novel heteronuclear bis-ligand namely 5-[4-(2-carboxyphenyl carbonyl amino)-phenyl-4-carbonyl methyl amino)-8-hydroxyquinoline was synthesized and characterized. This Bis-ligand was designated as CPHQ. Co-ordination polymers of this CPHQ bis-ligand were prepared with Cu+², Co+², Ni+², Mn+² and Zn+² metal ions. All of these Co-ordination polymers and the CPHQ ligand were characterized by elemental analysis, IR, NMR spectral studies, thermogravimetry, electronic reflectance spectral studies and magnetic susceptibility measurement. The synthesized novel Bis-ligand and their Co-ordination polymers were screened for their antimicrobial activity.
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