Resumen de Diamagnetic Anisotropy:: Two Iron Complexes as Laboratory Examples
Ignacio Fernandez de las Nieves, Jorge Fernando Fernández Sánchez
There are relatively few experiments describing the NMR properties of bis(amine) iron(II) phthalocyanine complexes. Several features make this experiment attractive: First, it nicely illustrates the diamagnetic anisotropy phenomena, providing both students and teachers an opportunity to gain insight into aspects such as phase correction and integration. Second, it gives the students hands-on experience with the NMR spectrometer and general aspects of one- and two-dimensional spectra processing. Finally, inorganic coordination synthetic work is needed and proved to be simple and high yielding.
